tag:blogger.com,1999:blog-3300702123878659843.post2757433184656969197..comments2024-03-26T05:25:50.831-04:00Comments on University of Ottawa NMR Facility Blog: Running NMR Spectra of Solids in an NMR Probe for LiquidsGlenn Faceyhttp://www.blogger.com/profile/05146575170575279335noreply@blogger.comBlogger2125tag:blogger.com,1999:blog-3300702123878659843.post-90826746302666560432008-06-05T08:31:00.000-04:002008-06-05T08:31:00.000-04:00nmrfreak,I had a similar experience with the same ...nmrfreak,<BR/><BR/>I had a similar experience with the same 10 mm BB probe on that Nicolet 360 back in 1983. I ran the solid state 77Se and 2H NMR spectra od H2Se, HDSe and D2Se at low temperature to observe the phase transitions. Collecting that data really made an impression on me. From T1 experiments, we found that the molecules in the plastically crystalline solid phase move faster than those in the liquid state. I think that is what really go me interested in NMR.Glenn Faceyhttps://www.blogger.com/profile/05146575170575279335noreply@blogger.comtag:blogger.com,1999:blog-3300702123878659843.post-26361826008390727412008-06-05T08:02:00.000-04:002008-06-05T08:02:00.000-04:00Glenn, your readers might be interested to know th...Glenn, your readers might be interested to know that one of the first experiments I did on our Nicolet 360 was to measure the Pb-207 shielding powder pattern for a lead salt (which salt escapes me - no protons around obviously). The important point for your post is that it was measured with a 10 mm high-resolution BB probe...and gave a beautiful result! The principal components of the shielding tensor were easily obtained.<BR/><BR/>MikeAnonymousnoreply@blogger.com